ARALDITE® CY 5980 / HARDENER HY 5980 / FLEXIBILIZER DY 040 / ACCELERATOR DY 061 / Filler Silica flour

ARALDITE® CY 5980 / HARDENER HY 5980 / FLEXIBILIZER DY 040 / ACCELERATOR DY 061 / Filler Silica flour is a liquid, flexibilized, hot-curing casting resin system, specifically designed for Class H dry-type distribution transformers, offering excellent electrical and mechanical properties.

RTU Product Type: Casting Resin

Product End Uses: Dry Type Distribution Transformers

Chemical Family: Epoxy & Epoxy Derivatives

Composites Processing Methods: Vacuum Casting

Features: Excellent Thermal Properties, Good Electrical Properties, Good Mechanical Properties, High Thermal Endurance

Cure Method: Heat Cure

Enhanced TDS

Identification & Functionality

Chemical Family
Fillers Included
RTU Product Type
Technologies
Product Families

Features & Benefits

Ready-to-Use Product Features
Features and Benefits
  • Good mechanical and electrical end properties.
  • Very high thermal endurance properties.
  • Class H according to IEC 60085.

Applications & Uses

Composites End Use
Composites Processing Methods
Cure Method
Product End Uses
Markets
Applications
Processing Information

The effective pot-life of the mix is about 1 day at temperatures below 25°C. Conventional batch mixers should be cleaned once a week or at the end of work. For longer interruptions of work, the pipes of the mixing and metering installations have to be cooled and cleaned with the resin component to prevent sedimentation and/or undesired viscosity increase. Interruptions over a week-end (approx. 48h) without cleaning are possible if the pipes are cooled at temperatures below 18°C. In case to use mixtures with high reactivity, we recommend to clean daily with the flexibiliser DY 040. Viscosity increase and gel time at various temperatures, refer Page 4.


Mold temperature
Conventional vacuum casting 60 - 100°C


Demolding times (depending on mold temperature and casting volume)
Conventional vacuum casting 4 - 8 h


Cure conditions (minimal postcure)
Conventional Vacuum Casting 6h at 80°C + 10h at 130°C or 6h at 80°C + 6h at 140°C

 

Castings with big volume (exothermic reaction, internal mechanical stresses) or encapsulations of heat sensitive active parts could be cured at appr. 80°C. To determine whether crosslinking has been carried to completion and the final proper- ties are optimal, it is necessary to carry out relevant measurements on the actual object or to measure the glass transition temperature. Different gelling and cure cycles in the manufacturing process could lead to a different crosslinking and glass transition temperature respectively.

 

Processing Viscosities

 

ARALDITE® CY 5980 / ARADUR® HY 5980 / FLEXIBILIZER DY 040 / ACCELERATOR DY 5985 / Filler Silica flour - Processing Information - 1

Fig4.1: Viscosity increase at 40, 60 and 80°C with DY 061, (1 pbw) (measurements with Rheomat 115) (Shear rate D = 10 s ⁻¹)

 

ARALDITE® CY 5980 / ARADUR® HY 5980 / FLEXIBILIZER DY 040 / ACCELERATOR DY 5985 / Filler Silica flour - Processing Information - 1

Fig.4.2 Initial viscosity as a function of temperature with DY 061, (1 pbw) (measurements with Rheomat 115 A MS DIN 125, D =10 s⁻¹)

 

ARALDITE® CY 5980 / ARADUR® HY 5980 / FLEXIBILIZER DY 040 / ACCELERATOR DY 5985 / Filler Silica flour - Processing Information - 1

Fig.4.3 Viscosity increase at 60 and 80°C with DY 062, (0.2 pbw) (measurements with Rheomat 115) (Shear rate D = 10 s⁻¹)

 

Gelation-/Cure Times

 

ARALDITE® CY 5980 / ARADUR® HY 5980 / FLEXIBILIZER DY 040 / ACCELERATOR DY 5985 / Filler Silica flour - Processing Information - 1

Fig.4.4 Geltime measured in function of temperature with DY 061, (1 pbw) (measurements with Gelnorm Instrument / ISO 9396)

 

ARALDITE® CY 5980 / ARADUR® HY 5980 / FLEXIBILIZER DY 040 / ACCELERATOR DY 5985 / Filler Silica flour - Processing Information - 1

Fig.4.5 Geltime measured in function of temperature with DY 062, (0.2 pbw) (measurements with Gelnorm Instrument / ISO 9396)

 

Mechanical and Physical Properties

 

Key Value Unit Test Method Condition
Tensile strength 75 - 85 MPa ISO 527

Cured for 6h at 80°C + 10h at 130°C

Elongation at break 1.0 - 1.2 % ISO 527

Cured for 6h at 80°C + 10h at 130°C

E modulus from tensile test 11,500 - 12,500 MPa ISO 527

Cured for 6h at 80°C + 10h at 130°C

Flexural strength 130 - 140 MPa ISO 178

Cured for 6h at 80°C + 10h at 130°C

Surface strain 1.3 - 1.5 % ISO 178

Cured for 6h at 80°C + 10h at 130°C

Compressive strength 170 - 190 MPa ISO 604

Cured for 6h at 80°C + 10h at 130°C

Compression set 14 - 16 % ISO 604

Cured for 6h at 80°C + 10h at 130°C

Impact strength (Charpy) 11 - 13 kJ/m² ISO 179

Cured for 6h at 80°C + 10h at 130°C

Critical stress intensity factor (K1c) 2.9 - 3.1 MPa·m¹/² CG 216-0/89

Cured for 6h at 80°C + 10h at 130°C

Specific fracture energy (G1c) 700 - 800 J/m² CG 216-0/89

Cured for 6h at 80°C + 10h at 130°C

Glass transition temperature (DSC) 60 - 80 °C ISO 11357-2

Cured for 6h at 80°C + 10h at 130°C

Coefficient of linear thermal expansion (Mean value for temperature range: 25 - 55°C) 34 - 40 x10⁻⁶ K⁻¹ ISO 11359-2

Cured for 6h at 80°C + 10h at 130°C

Thermal conductivity 0.8 - 0.9 W/m·K Similar to ISO 8894-1

Cured for 6h at 80°C + 10h at 130°C

Glow resistance 2b Class DIN 53459

Cured for 6h at 80°C + 10h at 130°C

Flammability (Thickness of specimen: 4 mm) HB   UL 94

Cured for 6h at 80°C + 10h at 130°C

Flammability (Thickness of specimen: 12 mm) V1   UL 94

Cured for 6h at 80°C + 10h at 130°C

Thermal endurance profile (TEP) See page 7   IEC 60216

Cured for 6h at 80°C + 10h at 130°C

Temperature index (TI): flexural strength (20,000h/10,000h) 180/197 °C IEC 60085

Cured for 6h at 80°C + 10h at 130°C

Thermal ageing class (20,000h) H   IEC 60085

Cured for 6h at 80°C + 10h at 130°C

Water absorption (10 days at 23°C) 0.06 - 0.08 % by wt ISO 62

Cured for 6h at 80°C + 10h at 130°C

Water absorption (60 minutes at 100°C) 0.10 - 0.15 % by wt ISO 62

Cured for 6h at 80°C + 10h at 130°C

Decomposition temperature (TGA) > 350 °C DTA

Cured for 6h at 80°C + 10h at 130°C

Density (Filler load: 66% by wt.) 1.80 - 1.90 g/cm³ ISO 1183

Cured for 6h at 80°C + 10h at 130°C

 

Electrical Properties

 

Key Value Unit Test Method Condition
Breakdown strength (IEC 60243-1) 20 - 24 kV/mm IEC 60243-1

Cured for 6h at 80°C + 10h at 130°C

Diffusion breakdown strength (DIN/VDE 0441/1) HD - 2 Class DIN VDE 0441-1

Cured for 6h at 80°C + 10h at 130°C

Temperature of specimen after test 23 °C N/A

Cured for 6h at 80°C + 10h at 130°C

HV arc resistance (IEC 61621) 183 - 185 sec IEC 61621

Cured for 6h at 80°C + 10h at 130°C

Tracking resistance (IEC 60112) CTI > 600 - 0.0   IEC 60112

Cured for 6h at 80°C + 10h at 130°C

Tracking resistance (with test solution B)

CTI > 600M - 0.0

  IEC 60112

Cured for 6h at 80°C + 10h at 130°C

Electrolytic corrosion (IEC 60426) A - 1 Grade IEC 60426

Cured for 6h at 80°C + 10h at 130°C

 

 

ARALDITE® CY 5980 / ARADUR® HY 5980 / FLEXIBILIZER DY 040 / ACCELERATOR DY 5985 / Filler Silica flour - Processing Information - 1

Fig.6.1: Loss factor (tan δ) and dielectric constant (εr) as a function of temperature (measurement frequency: 50 Hz / IEC 60250)


ARALDITE® CY 5980 / ARADUR® HY 5980 / FLEXIBILIZER DY 040 / ACCELERATOR DY 5985 / Filler Silica flour - Processing Information - 1

Fig.6.2: Volume resistivity (ρ) as a function of temperature (measurement voltage: 1000 V / IEC 60093)

 

Thermal Endurance

 

Investigated property:

Flexural strength (ISO 178)

Selected end point:

50% of initial value (144.3 MPa)

TI (HIC) 180 (17)

Statistical test variables:

 
CHI² 3.03
F= 1.5
Lower 95% confidence curve TC: 179°C

 

 

ARALDITE® CY 5980 / ARADUR® HY 5980 / FLEXIBILIZER DY 040 / ACCELERATOR DY 5985 / Filler Silica flour - Processing Information - 1

Fig. 7.1 With the high temperature index given above the materials qualify for use in systems with a thermal class of 180 C. This makes it suitable for designing and producing of class H cast resin distribution transformers.

Application Information

Dry-type distribution transformers.

System Preparation

General instructions for preparing liquid resin systems.

  • Long pot life is desirable in the processing of any casting resin system. Mix all of the components together very thoroughly at room temperature or slightly above and under vacuum. Intensive wetting of the filler is extremely important. Proper mixing will result in:
  1. Better flow properties and reduced tendency to shrinkage
  2. Lower internal stresses and therefore improved mechanical properties on object
  3. Improved partial discharge behaviour in high voltage applications.
  • For the mixing of medium to high viscous casting resin systems and for mixing at lower temperatures, we recommend special thin film degassing mixers that may produce additional self-heating of 10-15 K as a result of friction. For low viscous casting resin systems, conventional anchor mixers are usually sufficient.
  • In larger plants, two pre-mixers are used to mix the individual components with the respective quantities of fillers and additives under vacuum. Metering pumps then feed these premixes to the final mixer or a continuous mixer. The individual premixes can be stored at elevated temperature (about 60°C) for up to about 1 week, de-pending on formulation. Intermittent agitation during storage is advisable to prevent filler sedimentation.
  • Note: A premix of accelerator with resin is not stable; a premix of accelerator with hardener is stable under certain conditions. Please contact our staff for details
  • Mixing time can vary from 0.5 to 3 hours, depending on mixing temperature, quantity, mixing equipment and the particular application. The required vacuum is 0.5 to 8 mbar. Degassing time is recommended at least 1 hour. The vapour pressure of the individual components should be taken into account.
  • In the case of dielectrically highly stressed parts, we recommend checking the quality consistency and pre-drying of the filler. Their moisture content should be <0.2%.

Properties

Physical Form
Notes

* - Aradur HY 5980 is sensitive to humidity and tends to crystallise at low storage temperature. It can be re-liquefied by stirring and heating it to 40 - 80°C.

Regulatory & Compliance

Quality Standards

Storage & Handling

Storage Conditions

Store the components in a dry place according to the storage conditions stated on the label in tightly sealed original containers. Under these conditions, the shelf life will correspond to the expiry date stated on the label. After this date, the product may be processed only after reanalysis. Partly emptied containers should be tightly closed immediately after use. For information on waste disposal and hazardous products of decomposition in the event of a fire,

Other

Application Information
ValueUnitsTest Method / Conditions
Mix Ratio0.01 %(W)%(W)Accelerator : Resin
Mix Ratio4.1 %(W)%(W)Filler : Resin
Mix Ratio0.15 %(W)%(W)Flexibilizer : Resin
Mix Ratio0.95 %(W)%(W)Hardener : Resin