ARALDITE® CY 5980 / ARADUR® HY 5980 / FLEXIBILIZER DY 040 / ACCELERATOR DY 5985 / Filler Silica flour

ARALDITE® CY 5980 / ARADUR® HY 5980 / FLEXIBILIZER DY 040 / ACCELERATOR DY 5985 / Filler Silica flour is a liquid, flexibilized, hot-curing impregnating resin system designed for producing dry-type distribution transformers with excellent electrical and mechanical properties, suitable for Class H. Ideal for electrical insulation materials.

RTU Product Type: Impregnating Resin System

Product End Uses: Dry Type Distribution Transformers, Glass Fiber-Reinforced

Chemical Family: Epoxy & Epoxy Derivatives

Composites Processing Methods: Vacuum Pressure Impregnation (VPI)

Features: Good Electrical Properties, Good Mechanical Properties

Cure Method: Heat Cure

Enhanced TDS

Identification & Functionality

Features & Benefits

Ready-to-Use Product Features
Features and Benefits
  • Good mechanical and electrical end properties.
  • Very high thermal endurance properties.
  • Class H according to IEC 60085.

Applications & Uses

Composites Processing Methods
Cure Method
Product End Uses
System Preparation

General instructions for preparing liquid resin systems.

  • Long pot life is desirable in the processing of any casting resin system. Mix all of the components together very thoroughly at room temperature or slightly above and under vacuum. Intensive wetting of the filler is extremely important. Proper mixing will result in:
  1. Better flow properties and reduced tendency to shrinkage
  2. Lower internal stresses and therefore improved mechanical properties on object
  3. Improved partial discharge behaviour in high voltage applications.
  • For the mixing of medium to high viscous casting resin systems and for mixing at lower temperatures, we recommend special thin film degassing mixers that may produce additional self-heating of 10-15 K as a result of friction. For low viscous casting resin systems, conventional anchor mixers are usually sufficient.
  • In larger plants, two pre-mixers are used to mix the individual components with the respective quantities of fillers and additives under vacuum. Metering pumps then feed these premixes to the final mixer or a continuous mixer. The individual premixes can be stored at elevated temperature (about 60°C) for up to about 1 week, de-pending on formulation. Intermittent agitation during storage is advisable to prevent filler sedimentation.
  • Mixing time can vary from 0.5 to 3 hours, depending on mixing temperature, quantity, mixing equipment and the particular application. The required vacuum is 0.5 to 8 mbar. Degassing time is recommended at least 1 hour. The vapour pressure of the individual components should be taken into account.
  • In the case of dielectrically highly stressed parts, we recommend checking the quality consistency and pre-drying of the filler. Their moisture content should be <0.2%.

 

Application Information

Dry-type distribution transformers, glass fiber reinforced.

Processing Information

The effective pot-life is about 1 day at temperature below 25°C. Conventional batch mixers should be cleaned once a week or at the end of work. For longer interruptions of work, the pipes of the mixing and metering installations have to be cooled and cleaned to prevent sedimentation and/or undesired viscosity increase. Interruptions over a weekend (approx. 48h) without cleaning are possible if the pipes are cooled at temperature below 18°C. In case to use mixtures with high reactivity, we recommend to clean daily with the Flexibilizer DY 040 CI. Viscosity increase and gel time at various temperatures, refer to Figs: 4


Mold temperature
Conventional vacuum casting 80 - 100°C


Demolding times (depending on mold temperature and casting volume)
Conventional vacuum casting 4 - 8h
 

Cure conditions (minimal postcure)
Conventional vacuum casting

4h at 80°C + 10h at 130°C
4h at 80°C + 6h at 140°C

Castings with big volume (exothermic reaction, internal mechanical stresses) or encapsulations of heat sensitive active parts could be cured at appr. 80°C. To determine whether crosslinking has been carried to completion and the final proper- ties are optimal, it is necessary to carry out relevant measurements on the actual object or to measure the glass transition temperature. Different gel and postcuring cycles in the manufacturing process could influence the crosslinking and the glass transition temperature respectively.

 

ARALDITE® CY 5980 / ARADUR® HY 5980 / ACCELERATOR DY 061 - Processing Information - 1

Fig.4.1: Viscosity increase at 60 and 80°C (measurements with Rheomat 115) (Shear rate D = 10S⁻¹)

 

ARALDITE® CY 5980 / ARADUR® HY 5980 / ACCELERATOR DY 061 - Processing Information - 1

Fig.4.2: Initial viscosity in function of temperature (measurements with Rheomat 115, D = 10S⁻¹)

 

ARALDITE® CY 5980 / ARADUR® HY 5980 / ACCELERATOR DY 061 - Processing Information - 1

Fig.4.4: Geltime measured in function of temperature (measurement with Gelnorm Instrument)

 

Mechanical and Physical properties

 

Key Value Unit Test Method Condition
Tensile strength 70 - 80 MPa ISO R 527

Cured for 6h at 80°C + 10h at 130°C

Elongation at break 0.9 - 1.1 % ISO R 527

Cured for 6h at 80°C + 10h at 130°C

E-Modulus from tensile test 12,000 - 12,400 MPa ISO R 527

Cured for 6h at 80°C + 10h at 130°C

Flexural strength at 23°C 120 - 125 MPa ISO 178

Cured for 6h at 80°C + 10h at 130°C

Surface strain at 23°C 1.0 - 1.5 % ISO 178

Cured for 6h at 80°C + 10h at 130°C

E modulus from flexural test 12,300 - 14,000 MPa ISO 178

Cured for 6h at 80°C + 10h at 130°C

Critical stress intensity factor (KIC) 2.7 - 2.9 MPa·m¹/² CG 216-0/89

Cured for 6h at 80°C + 10h at 130°C

Specific energy at break (GIC) 600 - 620 kJ/m² CG 216-0/89

Cured for 6h at 80°C + 10h at 130°C

Glass transition temperature (DSC) 65 - 75 °C IEC 61006

Cured for 6h at 80°C + 10h at 130°C

Coefficient of linear thermal expansion (20 - 60°C) 35 - 37 x 10⁻⁶ K⁻¹ DIN 53752

Cured for 6h at 80°C + 10h at 130°C

Thermal endurance profile (TEP) Fig 7   DIN/IEC 60216

Cured for 6h at 80°C + 10h at 130°C

Temperature index (TI): flexural strength (20,000h/10,000h) 180/195 °C IEC 60085

Cured for 6h at 80°C + 10h at 130°C

Thermal ageing class (20,000h) Class H   IEC 60085

Cured for 6h at 80°C + 10h at 130°C

Water absorption (10 days at 23°C) 0.1 - 0.2 % by wt ISO 62

Cured for 6h at 80°C + 10h at 130°C

Water absorption (60 minutes at 100°C) 0.1 - 0.2 % by wt ISO 62

Cured for 6h at 80°C + 10h at 130°C

Density (Filler load: 66% by wt.) 1.8 - 1.9 g/cm³ DIN 55990

Cured for 6h at 80°C + 10h at 130°C

 

Electrical Properties

 

Key Value Unit Test Method Condition
Breakdown strength (IEC 60243-1) 18 - 22 kV/mm IEC 60243-1

Cured for 6h at 80°C + 10h at 130°C

HV arc resistance (ASTM D 495) 185 - 195 sec ASTM D 495

Cured for 6h at 80°C + 10h at 130°C

Tracking resistance (with solution A) CTI > 600 - 0.0   IEC 60112

Cured for 6h at 80°C + 10h at 130°C

Tracking resistance (with solution B)

CTI > 600M - 0.0

  IEC 60112

Cured for 6h at 80°C + 10h at 130°C

Electrolytic corrosion (DIN 53489) A-1 Grade DIN 53489

Cured for 6h at 80°C + 10h at 130°C

 

ARALDITE® CY 5980 / ARADUR® HY 5980 / ACCELERATOR DY 061 - Processing Information - 1

Fig.6.1: Loss factor (tan𝛿) and dielectric constant (𝜀𝑟) as a function of temperature (measurement frequency: 50 Hz) (IEC 250 / DIN 53483)

 

ARALDITE® CY 5980 / ARADUR® HY 5980 / ACCELERATOR DY 061 - Processing Information - 1

Fig.6.2: Volume resistivity (ρ) as a function of temperature (measurement voltage: 1000 V) (IEC 93 / DIN 53482)

 

Thermal Endurance Profile acc. IEC 60216
Investigated Flexural strength (ISO 178)
Results 20000h at 180°C
10000h at 195°C
Selected end 50% of initial value


ARALDITE® CY 5980 / ARADUR® HY 5980 / ACCELERATOR DY 061 - Processing Information - 1

Fig. 7 With the high temperature index given above the materials qualifies for use in systems with a thermal class of 180°C. This makes it suitable for designing and producing of class H cast resin distribution transformers.

Properties

Physical Form
Notes

Aradur HY 5980 is sensitive to humidity and tends to crystallise at low storage temperature. It can be re-liquefied by stirring and heating it to 40 - 80°C.

Regulatory & Compliance

Quality Standards

Safety & Health

Handling Precautions

Protective clothing

Yes
Gloves Essential
Arm protector

Recommended when skin contact likely

Goggestery diasses

Yes

Respirator/dust mask

Recommended

Skin protection before starting work

Apply barrier cream to exposed skin

Skin protection after washing

Apply barrier or nourishing cream

Skin protection cleansing of contaminated skin

Dab off with absorbent paper, wash with warm water and alkali-free soap, then dry with disposable towels. Do not use solvents

Clean shop requirements

Cover workbenches, etc. with light coloured paper. Use disposable breakers, etc.

Disposal of spillage

Soak up with sawdust or cotton waste and deposit in plastic-lined bin

Ventilation: of workshop

Renew air 3 to 5 times an hour

Ventilation: of workplace

Exhaust fans. Operatives should avoid inhaling vapours.

Industrial Hygiene

Mandatory and recommended industrial hygiene procedures should be followed whenever our products are being handled and processed.

First Aid Information
  • Contamination of the eyes by resin, hardener or casting mix should be treated immediately by flushing with clean, running water for 10 to 15 minutes. A doctor should then be consulted.
  • Material smeared or splashed on the skin should be dabbed off, and the contaminated area then washed and treated with a cleansing cream (see above). A doctor should be consulted in the event of severe irritation or burns. Contaminated clothing should be changed immediately.
  • Anyone taken ill after inhaling vapours should be moved out of doors immediately.

Storage & Handling

Storage Conditions

Store the components at 18 - 25°C, in tightly sealed and dry in the original containers. Under these conditions, the shelf life will correspond to the expiry date stated on the label. After this date, the product may be processed only following reanalysis. Partly emptied containers should be closed tightly immediately after use. For information on waste disposal and hazardous products of decomposition in the event of fire.

Other

Application Information
ValueUnitsTest Method / Conditions
Mix Ratio0.02 %(W)%(W)Accelerator : Resin
Mix Ratio4.1 %(W)%(W)Filler : Resin
Mix Ratio0.13 %(W)%(W)Flexibilizer : Resin
Mix Ratio0.95 %(W)%(W)Hardener : Resin